Hydrogen embrittlement is prevented in Sm.sub.2Co.sub.17-based magnets and R.sub.2Fe.sub.14B-based magnets by metal plating the magnet, then carrying out heat treatment, or by forming a metal oxide or metal nitride layer on the metal plating layer or directly on the magnet itself.

 
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> Preparation of a high purity and high concentration hydroxylamine free base

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