Provided are methods for producing pentahalosulfur peroxides and monoxides, such as bis-(pentafluorosulfur) peroxide, that involve exposing a composition comprising a pentahalosulfur hypohalite, and optionally a sulfur hexahalide or trihalomethyl hypohalite, to a halogen free radical scavenger.

 
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> Auto-oxidation production of hydrogen peroxide via oxidation in a microreactor

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